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Modulated Temperature Differential Scanning Calorimetry : Theoretical and Practical Applications in Polymer Characterisation. 1st ed. 2006

種類:
電子ブック
責任表示:
edited by Mike Reading, Douglas J. Hourston
出版情報:
Dordrecht : Springer Netherlands : Imprint: Springer, 2006
著者名:
シリーズ名:
Hot Topics in Thermal Analysis and Calorimetry ; 6
ISBN:
9781402037504 [1402037503]  CiNii Books  Calil
注記:
Theory and Practice of Modulated Temperature Differential Scanning Calorimetry -- The Application of Modulated Temperature Differential Scanning Calorimetry for the Characterisation of Curing Systems -- Applications of Modulated Temperature Differential Scanning Calorimetry to Polymer Blends and Related Systems -- The Application of MTDSC to Polymer Melting.
MTDSC provides a step-change increase in the power of calorimetry to characterize virtually all polymer systems including curing systems, blends and semicrystalline polymers. It enables hidden transitions to be revealed, miscibility to be accurately assessed, and phases and interfaces in complex blends to be quantified. It also enables crystallinity in complex systems to be measured and provides new insights into melting behaviour. All of this is achieved by a simple modification of conventional DSC. In 1992 a new calorimetric technique was introduced that superimposed a small modulation on top of the conventional linear temperature program typically used in differential scanning calorimetry. This was combined with a method of data analysis that enabled the sample’s response to the linear component of the temperature program to be separated from its response to the periodic component. In this way, for the first time, a signal equivalent to that of conventional DSC was obtained simultaneously with a measure of
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